PRELIMINARY STUDIES ON PROTECTION OF CARBONYL COMPOUNDS USING ANHYDROUS SALT-SILICA MIXTURE
Abstract
Some cheap, non-corrosive, and environmentally friendly inorganic salts were immobilised on silica to afford homogenous mixtures which were employed to mediate the protection of carbonyl functionality with ethylene glycol in the absence of solvent. The methodology proved to be feasible with the successful acetalisation and ketalisation of all the compounds albeit with fair to low yields.
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